TY - JOUR
T1 - Bis[(methylsulfanyl)carbonyl]disulfane
AU - Ford, David K.
AU - Young, Victor G.
AU - Barany, George
N1 - Copyright:
Copyright 2013 Elsevier B.V., All rights reserved.
PY - 2012/7
Y1 - 2012/7
N2 - The title compound, C4H6O2S4, was prepared by repeating, with subtle improvements, a multi-step route originally described by Mott & Barany [J. Chem. Soc. Perkin Trans. 1 (1984), pp. 2615-2621]. The title compound was obtained for the first time as a crystalline material. The two [(methylsulfanyl)carbonyl]sulfenyl moieties are essentially perpendic-ular to each other, each approximately planar (r.m.s. deviations of 0.02 and 0.01 Å) and with a C - S - S - C torsion angle = 90.99 (6)°, which compares well with the theoretical value of 90°.
AB - The title compound, C4H6O2S4, was prepared by repeating, with subtle improvements, a multi-step route originally described by Mott & Barany [J. Chem. Soc. Perkin Trans. 1 (1984), pp. 2615-2621]. The title compound was obtained for the first time as a crystalline material. The two [(methylsulfanyl)carbonyl]sulfenyl moieties are essentially perpendic-ular to each other, each approximately planar (r.m.s. deviations of 0.02 and 0.01 Å) and with a C - S - S - C torsion angle = 90.99 (6)°, which compares well with the theoretical value of 90°.
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U2 - 10.1107/S1600536812024750
DO - 10.1107/S1600536812024750
M3 - Article
C2 - 22798780
AN - SCOPUS:84863591225
SN - 1600-5368
VL - 68
SP - o2102
JO - Acta Crystallographica Section E: Structure Reports Online
JF - Acta Crystallographica Section E: Structure Reports Online
IS - 7
ER -