Effect of heat treatment on adhesion in the Cr/Al2O3 system

Sriram Viswanathan, David L. Kohlsted

Research output: Contribution to journalConference articlepeer-review

Abstract

Continuous microscratch experiments have been carried out to investigate the effect of various heat treatments on adhesion in the Cr/Al2O3 system. After samples were prepared by vapor depositing 0.32 μm thick Cr films on (1102) surfaces of single crystal sapphire substrates, they were annealed at different temperatures at controlled oxygen partial pressures. In the subsequent continuous microscratch tests, a conical diamond indenter with a 1 μm tip radius was driven simultaneously into and across the sample until a load drop occurred. Optical and scanning electron microscopy observations demonstrate that a portion of the Cr film delaminated from the Al2O3 substrate at that point. The interfacial strain energy release rate was calculated from the load at failure combined with the size and geometry of the delaminated region. The work of adhesion was found to decrease dramatically on annealing in an H2-Ar mixture at 250°C.

Original languageEnglish (US)
Pages (from-to)659-663
Number of pages5
JournalMaterials Research Society Symposium - Proceedings
Volume308
DOIs
StatePublished - 1993
EventProceedings of the 1993 Spring Meeting of the Materials Research Society - San Francisco, CA, USA
Duration: Apr 12 1993Apr 16 1993

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