Abstract
(Matrix Presented) The concentration of organolithium, organomagnesium halide, and lithium diisopropylamide solutions can be reliably determined using No-D NMR spectroscopy by integration against the added internal standard 1,5-cyclooctadiene (COD) (or cyclooctene). In addition, common impurities and degradation products can be assessed.
Original language | English (US) |
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Pages (from-to) | 2567-2570 |
Number of pages | 4 |
Journal | Organic Letters |
Volume | 6 |
Issue number | 15 |
DOIs | |
State | Published - Jul 22 2004 |