Synthesis of propionamide pyridine and pyridine N-oxide ligands

Iris Binyamin, Sylvie Pailloux, Benjamin P. Hay, Brian M. Rapko, Eileen N. Duesler, Robert T. Paine

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10 Scopus citations


(Chemical Equation Presented) A new set of pyridine and pyridine N-oxides functionalized with N,N-dimethylpropionamide pendant groups in the 2- and 2,6-positions have been prepared from the combination of 2-chloromethylpyridine and 2,6-bis(chloromethyl) pyridine with α-lithio N,N-dimethyl acetamide. The coordination interaction between 2-(N,N-dimethylpropionamide) pyridine N-oxide (10) and Tb(NO3)3 has been unambiguously defined via single crystal X-ray diffraction analysis of Tb(10)(NO3) 3(H2O).

Original languageEnglish (US)
Pages (from-to)99-103
Number of pages5
JournalJournal of Heterocyclic Chemistry
Issue number1
StatePublished - Jan 1 2007


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