A structural resolution cryo-TEM study of the early stages of MFI growth

Sandeep Kumar; Zhuopeng Wang; R. Lee Perm; Michael Tsapatsis

doi:10.1021/ja8063167

A structural resolution cryo-TEM study of the early stages of MFI growth

Sandeep Kumar, Zhuopeng Wang, R. Lee Perm, Michael Tsapatsis

Chemical Engineering and Materials Science

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104 Scopus citations

Abstract

Room-temperature aging of zeolite precursor silica sol was followed by SAXS and cryo-TEM. Cryo-TEM imaging of zeolite materials with structural resolution is demonstrated. The results suggest the formation of predominantly amorphous aggregates before MFI crystallization.

Original language	English (US)
Pages (from-to)	17284-17286
Number of pages	3
Journal	Journal of the American Chemical Society
Volume	130
Issue number	51
DOIs	https://doi.org/10.1021/ja8063167
State	Published - Dec 24 2008

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title = "A structural resolution cryo-TEM study of the early stages of MFI growth",

abstract = "Room-temperature aging of zeolite precursor silica sol was followed by SAXS and cryo-TEM. Cryo-TEM imaging of zeolite materials with structural resolution is demonstrated. The results suggest the formation of predominantly amorphous aggregates before MFI crystallization.",

author = "Sandeep Kumar and Zhuopeng Wang and {Lee Perm}, R. and Michael Tsapatsis",

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AU - Kumar, Sandeep

AU - Wang, Zhuopeng

AU - Lee Perm, R.

AU - Tsapatsis, Michael

PY - 2008/12/24

Y1 - 2008/12/24

N2 - Room-temperature aging of zeolite precursor silica sol was followed by SAXS and cryo-TEM. Cryo-TEM imaging of zeolite materials with structural resolution is demonstrated. The results suggest the formation of predominantly amorphous aggregates before MFI crystallization.

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A structural resolution cryo-TEM study of the early stages of MFI growth

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